Preconcentration of lead using solidification of floating organic drop and its determination by electrothermal atomic absorption spectrometry

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Preconcentration of lead using solidification of floating organic drop and its determination by electrothermal atomic absorption spectrometry

A simple microextraction method based on solidification of a floating organic drop (SFOD) was developed for preconcentration of lead prior to its determination by electrothermal atomic absorption spectrometry (ETAAS). Ammonium pyrolidinedithiocarbamate (APDC) was used as complexing agent, and the formed complex was extracted into a 20 μL of 1-undecanol. The extracted complex was diluted with et...

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dispersive liquid-liquid microextraction based on solidification of floating organic drop combined with flame atomic absorption spectrometry for preconcentration and determination of thallium(iii) in water samples

dispersive liquid-liquid microextraction technique based on solidification of a floating organic drop (dllme-sfo) combined with flame atomic absorption spectrometry was developed for determination of thallium in water sample. an appropriate mixture of acetone and 1-undecanol was rapidly injected into an aqueous sample containing tlcl4- which forms an ion pair with brilliant green reagent and as...

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ژورنال

عنوان ژورنال: Journal of Advanced Research

سال: 2013

ISSN: 2090-1232

DOI: 10.1016/j.jare.2012.07.002